hplc a practical user s guide

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Hplc

Author : Marvin C. McMaster
ISBN : 9780470079089
Genre : Science
File Size : 82. 50 MB
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This Second Edition of the classic handbook details how to set up an HPLC system that capitalizes on the latest innovations. It covers new techniques in high-temperature, micro-flow, and ultra-fast chromatography, the linking of an HPLC to a mass spectrometer, and more. Complete with a CD-ROM and appendices, this guide has everything chromatographers need to know to confidently separate, identify, purify, and quantify compounds. Note: CD-ROM/DVD and other supplementary materials are not included as part of eBook file.

Lc Ms

Author : Marvin C. McMaster
ISBN : 9780471736578
Genre : Science
File Size : 36. 37 MB
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A practical guide to using and maintaining an LC/MS system The combination of liquid chromatography (LC) and mass spectrometry(MS) has become the laboratory tool of choice for a broad range ofindustries that require the separation, analysis, and purificationof mixtures of organic compounds. LC/MS: A Practical User's Guide provides LC/MS users with aneasy-to-use, hands-on reference that focuses on the practicalapplications of LC/MS and introduces the equipment and techniquesneeded to use LC/MS successfully. Following a thorough explanationof the basic components and operation of the LC/MS system, theauthor presents empirical methods for optimizing the techniques,maintaining the instrumentation, and choosing the appropriate MS orLC/MS analyzer for any given problem. LC/MS covers everything users need to know about: The latest equipment, including quadrupole, time-of-flight, andion trap analyzers Cutting-edge processes, such as preparing HPLC mobile phasesand samples; handling and maintaining a wide variety of silica,zirconium, and polymeric separation columns; interpreting andquantifying mass spectral data; and using MS interfaces Current and future applications in the pharmaceutical andagrochemical industries, biotechnology, clinical research,environmental studies, and forensics An accompanying PowerPoint® slide-set on CD-ROM provides vitalteaching tools for instructors and new equipment operators.Abundantly illustrated and easily accessible, the text is designedto help students and practitioners acquire optimum proficiency inthis powerful and rapidly advancing analytical application.

Gc Ms

Author : Marvin C. McMaster
ISBN : 9781118210055
Genre : Science
File Size : 65. 39 MB
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Updated and expanded, the classic guide to GC/MS helps chromatographers quickly learn to use this technique for analyzing and identifying compounds. After explaining the fundamentals, it discusses optimizing, tuning, using, and maintaining GC/MS equipment; explores advances in miniaturized and field-portable GC/MS systems and microfluidic components; and more. Complete with a CD-ROM, it covers applications in the environmental laboratory and in forensics, toxicology, and space science. This is the premier resource for professionals in those fields and for students.

Der Hplc Experte

Author : Stavros Kromidas
ISBN : 9783527676583
Genre : Science
File Size : 64. 83 MB
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Der rasanten Entwicklung auf dem Gebiet der HPLC wird mit diesem Buch Rechnung getragen: Von Gradientenoptimierung über Kopplungs- und 2D-Techniken bis zu Dokumentation und Informationsbeschaffung - aktuell und kompakt geschrieben von Praktikern für Praktiker. Inhalt: 1 LC/MS-Kopplung 1.1 Stand der Technik in der LC/MS-Kopplung 1.2 Technische Aspekte und Fallstricke der LC/MS-Kopplung 1.3 LC/MS-Kopplung - ein praktisches Beispiel aus der Ionenchromatographie 2 HPLC-GC-Kopplung in der Praxis; Theorie, Applikationsbeispiele und Ausblick 3 Optimisierungsstrategien in der RP-HPLC 4 Der Gradient in der RP-Chromatographie 4.1 Aspekte der Gradienten-Optimierung 4.2 Vorhersagen von Gradienten 5 Vergleich und Auswahl von modernen HPLC-Säulen 6 Trenntechniken in der Biochromatographie 7 Moderne HPLC-Softwareprogramme - Eigenschaften, Vergleich, Ausblick 8 Möglichkeiten der "richtigen" Integration heute 9 HPLC im reglementierten Bereich 9.1 Intelligente Dokumentationen 9.2 Tipps für eine gelungene FDA-Inspektion 10 Effiziente Informationsbeschaffung im Zeitalter von Web 2.0 am Beispiel der HPLC 11 Trends in der Detektionstechnik

Encyclopedia Of Chromatography

Author : Jack Cazes
ISBN : 0824727878
Genre : Science
File Size : 39. 89 MB
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A guide to specific chromatographic techniques and principles. It offers basic introduction to the science and technology of the method, as well as references on the theory and methodology for analysis of specific chemicals and applications in a range of industries. It contains over 400 cross-referenced articles with more than 80 articles.

Hplc

Author : Toshihiko T Hanai
ISBN : 9781847551078
Genre : Science
File Size : 71. 79 MB
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How can these compounds be separated? Why was that method used? These are the two basic questions often asked by students of chromatography. HPLC: A Practical Guide provides the answers, enabling the reader to grasp the concepts of the technique using simple, representative chromatograms. Divided into six chapters, this practical guide covers basic concepts of HPLC; instrumentation; stationary phase materials; eluents; column efficiency; and the influence of physical chemistry on separations. Focusing on the basic considerations such as selection of stationary phase and eluent, rather than specific applications, sections on troubleshooting are also included. Uniquely, the descriptions of chromatographic separations are based on solubility using molecular properties, and solubility parameters are used to analyse the selections of chromatographic mode and column. Presenting the chemistry of liquid chromatography for undergraduate students, this valuable practical guide will also be useful for laboratory staff in industry and academia.

Buying And Selling Laboratory Instruments

Author : Marvin C. McMaster
ISBN : 1118031849
Genre : Science
File Size : 89. 12 MB
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A time-tested, systematic approach to the buying and selling of complex research instruments Searching for the best laboratory instruments and systems can be a daunting and expensive task. A poorly selected instrument can dramatically affect results produced and indirectly affect research papers, the quality of student training, and an investigator's chances for advancement. Buying and Selling Laboratory Instruments offers the valuable insights of an analytical chemist and consultant with over four decades of experience in locating instruments based upon both need and price. It helps all decision makers find the best equipment, service, and support while avoiding the brand-loyalty bias of sales representatives so you can fully meet your laboratory's requirements. The first section of the book guides buyers through the hurdles of funding, purchasing, and acquiring best-fit instruments at the least-expensive price. It explains how to find vendors that support their customers with both knowledgeable service and application support. Also offered is guidance on adapting your existing instruments to new applications, integrating new equipment, and what to do with instruments that can no longer serve in research mode. The second section explains the sales process in detail. This is provided both as a warning against manipulative sales reps and as a guide to making the sale a win-win process for you and your vendor. It also shows you how to select a knowledgeable technical guru to help determine the exact system configuration you need and where to find the best price for it. Added bonuses are summary figures of buying sequence and sales tools and an appendix containing frequently asked questions and memory aids. Buying and Selling Laboratory Instruments is for people directly involved in selecting and buying instruments for operational laboratories, from the principle investigator to the person actually delegated with investigating and selecting the system to be acquired. Sales representatives; laboratory managers; universities; pharmaceutical, biotech, and forensic research firms; corporate laboratories; graduate and postdoctoral students; and principle investigators will not want to be without this indispensible guide.

Analytische Chemie

Author : Georg Schwedt
ISBN : 9783527698790
Genre : Science
File Size : 58. 78 MB
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Alle relevanten Aspekte der Analytischen Chemie werden in diesem Lehrbuch, das gleichzeitig auch als Referenz für Praktiker dient, umfassend und klar auf den Punkt gebracht. Das Autorenteam wird durch zwei aktive und international bekannte Professoren verstärkt; dies sorgt für frischen Wind, gleichzeitig wird der didaktisch ausgefeilte Stil der Vorauflagen beibehalten. Von der Analysenstrategie zur Probenvorbereitung, von der Maßanalyse über spektroskopische und chromatographische Methoden bis zur Automatisierung - DAS Lehrbuch für alle, die sich mit Analytischer Chemie beschäftigen.

Hplc Troubleshooting

Author : Günter J. Eppert
ISBN : 3000108084
Genre :
File Size : 89. 71 MB
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Chromatography

Author : E. Heftmann
ISBN : 0080472249
Genre : Science
File Size : 68. 86 MB
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Chromatography has emerged as the most important and versatile analytical method. The book is not only an updated version of Heftmann's classical text, but it covers areas of future importance, such as microfluidics and computer resources. Under his experienced guidance, authorities in each field have contributed their practical experience to an integrated treatment of modern micro analysis. In Part A the theoretical basis of individual separation methods is explained and the technical aspects are illustrated. It includes the theory of gas and liquid chromatography as well as specific chromatographic techniques, such as size-exclusion, planar, ion, and affinity chromatography as well as various electrokinetic separation techniques. Microfluidics are covered for the first time and useful sources of analytical instruments are listed and evaluated. 1. Each chapter written by an authority 2. Thorough treatment of the theoretical basis of separation methods 3. Practical guide for performing analyses

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